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Place a spinvane and of magnesium turnings into an oven dried conical vial Attach the Claisen adapter to the conical vial. On the curved joint attach a drying tube filled with calcium chloride Place

Place a spinvane and of magnesium turnings into an oven dried  conical vial  Attach the Claisen adapter to the conical vial. On the curved joint attach a drying tube filled with calcium chloride Place a Teflon-rubber septum and screw cap on the straight portion of the adapter Clamp the appa-ratus so that it sits centered on a heater-stirrer no stirring at first and NO HEATING Measure nth of anhydrous diethyl ether in a second  conical vial and cap it You should use this diethy ether to make the solutions needed throughout this experiment  Weigh a conical

Mar 17 2020 Read more Less More

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